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2026-10-28

μGAS1001 Micro-Gas Reaction Evaluation System: The Core Instrument for Online Photocatalytic Gas Analysis | Perfectlight

Why Photocatalytic Experiments Cannot Do Without Online Gas Analysis

In reactions such as photocatalytic water splitting and CO₂ reduction, the target products are mostly gases (H₂, O₂, CO, CH₄, and so on). Traditional offline sampling requires stopping the light, collecting the gas, and then sending it to a chromatograph—this interrupts the photoreaction, introduces human error, and cannot capture the dynamic inflection point of product generation. The value of the μGAS1001 micro-gas reaction evaluation system is precisely to turn "reaction – sampling – detection" into a closed loop: the gas inside the reactor is automatically introduced into the gas chromatograph, peaks are quantified on a set cycle, and the entire process runs without manual intervention.

How μGAS1001 Works

The complete system consists of three parts: the photocatalytic reaction system provides a controlled light and atmosphere environment; the PLD-CGA1000 compound gas analyzer or sampling valve feeds the trace gas into the chromatographic column; and the gas chromatograph performs separation and quantification. The three are linked through tubing and a timed program, forming a loop of "photoreaction → online injection → chromatographic quantification → data feedback."

ModuleFunctionKey metrics
Photocatalytic reaction systemProvides light and a gas–solid / liquid–solid reaction environmentAir tightness, illumination uniformity
Injection & carrier-gas unitFeeds trace gas into the chromatographDead volume, response speed
Gas chromatographSeparates and quantifies each gas componentDetection limit, repeatability

Typical Application Scenarios

  • Photocatalytic water splitting (H₂ / O₂): plot the real-time H₂ production-rate curve and evaluate catalyst stability.
  • Photoelectrocatalytic CO₂ reduction: online distinction of CO, CH₄, and C₂ products to avoid product accumulation and contamination.
  • Photocatalytic activity evaluation: high-throughput gas reading when paired with multi-channel screening systems such as the PCX-50C.

Three Points to Watch When Building the System

  • Keep the tubing dead volume small; otherwise the response is slowed and the true inflection point is smoothed out.
  • Match the carrier-gas flow rate with the chromatography program to ensure integratable peak shapes.
  • Calibrate the reaction system and the detection end under a shared atmosphere. The PL-MW2000 high-intensity light power meter only calibrates light intensity at the sample position; gas quantification requires calibrating the chromatograph response factor with standard gas.

Free consultation: Want to upgrade your photocatalysis platform into a closed-loop online analysis system? Tell us your reaction system (gas–solid / liquid–solid) and target products, and Perfectlight application engineers will help you assemble the μGAS1001, gas chromatograph, and calibration plan.

Tel: 400-1161-365 / 010-62128921 Perfectlight Official Website

Related Products & Resources

Frequently Asked Questions (FAQ)

What is the relationship between μGAS1001 and the gas chromatograph?

The μGAS1001 is the complete micro-gas reaction evaluation system, while the gas chromatograph is its detection unit. The system links the photocatalytic reactor, injection valve, and gas chromatograph to achieve automatic quantification of produced gas.

What are the advantages of online analysis over offline analysis?

Online analysis does not interrupt the photoreaction, programmatic injection eliminates human error, and it continuously records how products change over time—making it far easier to capture kinetic inflection points.

Do I have to buy the complete system to build the closed loop?

The reactor, injection, and chromatograph must be linked together. Perfectlight offers the complete μGAS1001 package and also supports integration with existing modules such as the PCX-50C and PLD-CGA1000.

This article does not constitute a performance commitment; specific technical parameters are subject to the actual product documentation and mutual confirmation.

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