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photothermocatalytic光热催化反应系统

Rapid-heating multi-field fixed-bed reactor

Column:光热催化反应系统Brand:PerfectlightViews:109
Rapid-heating multi-field fixed-bed reactor
  • Introduction
  • Application
  • Literature
  • Maintenance

The rapid-heating multi-field fixed-bed reactor aims to construct field-strengthened and flexibly coupled multi-field interactions. By altering catalytic reaction pathways in multiple dimensions—such as electronic-state regulation, reaction kinetics optimization, and mass-transport enhancement—it achieves a synergistic enhancement effect of “1+1>2”.

Innovative Breakthroughs

● Light utilization efficiency: increased by approximately 60% or more (compared with a top-illumination light-guide-column structure)

The top-illumination photothermal reactor has a light utilization efficiency of approximately 50%.

This reactor has a light utilization efficiency of approximately 80%.

Overall efficiency improved by approximately 60% or more.

● Electric-heat utilization efficiency: increased by approximately 3 times or more (compared with conventional tubular furnace systems)

A tubular heating furnace requires about 130–150 W to maintain 500℃ under no-load conditions.

This reactor requires about 40 W to maintain 500℃ under no-load test conditions.

Overall electrical energy utilization can be improved by about three times or more.

● Experimental time efficiency: increased by several times or more (compared with traditional fixed-bed systems)

Conventional fixed-bed systems are time-consuming due to slow heating/cooling balance; temperature adjustments or catalyst screening take time, and cooling typically requires next-day operations.

This reactor heats and cools rapidly, with thermal equilibrium reached in about 15 minutes, allowing up to 8 or more samples per day.

Overall time efficiency can be improved by several times or more.

Enables single-wavelength, high-energy-density photothermal coupled catalytic reactions;

Implements coupling strategies between microwave fields and catalysts (e.g., heterojunction catalyst design) and has developed an integrated multi-field reactor combining light, heat, and microwaves;

Developed solutions for hard-to-degrade problems in industrial waste gas and chemical exhaust streams.

Distinctive Advantages

● Feature 1: Multi-energy-field coupling

Light field, resistive heating field, microwave field—study catalytic reactions under different individual or synergistic fields, such as light–heat coupling, light–microwave coupling, and light–heat–microwave multi-field coupling.

● Feature 2: Rapid-heating characteristics

① Resistive heating temperature rise rate: ≈100℃/min; ② Microwave heating temperature rise rate: ≈40–50℃/min; ③ Light-source heating temperature rise rate: ≈20℃/min;

High experimental efficiency and suitability for fast-heating reaction requirements.

● Feature 3: Fast response

① Fast thermal equilibrium (~15 min), improving heating-balance time by over ~3× compared with traditional heating; ② The reaction zone has a small void volume with almost no dead volume, enabling efficient gas exchange and very short reaction response times (on the order of seconds), showing significant improvement over conventional tubular reactors.

● Feature 4: High efficiency and energy saving

Light source: annular-illumination design places the light source close to the reactor, minimizing optical path loss; the reactor includes an internal reflective layer to improve secondary utilization of reflected light.

Resistive heating: ① Built-in heating elements with catalyst in close contact with the heater to effectively reduce conductive heat loss; ② Vacuum insulation layer design reduces air thermal conductivity (heat-conduction coefficient less than 1/100 of that at atmospheric pressure); ③ Reactor internal reflective layer enables secondary utilization of thermal infrared; compared with traditional reaction furnaces, maintenance energy consumption is reduced by over three times.

● Feature 5: Light energy utilization

① Single-wavelength LED source enables precise light control, matching catalyst bandgaps, avoiding multi-wavelength interference, and improving quantum efficiency.

② The irradiated area is greatly increased and monochromatic light power density is relatively high; the catalyst surface can reach up to roughly 32 suns. Effective illuminated area ranges from 3.14 cm2 (bed height 10 mm) to 15.7 cm2 (bed height 50 mm), with a maximum illuminated area of about 31.4 cm2. For example, the HL100-365 light source has a light power density >3.2 W/cm2 (measured without mesh shielding).

Applications

Thermal–light–microwave multi-field coupling

Thermal–light coupling

Resistive heating field

Thermal–microwave coupling

Light energy field

Light–microwave coupling

Microwave energy field

Technical Parameters

Type Performance Parameters Remarks
Device model Rapid-heating multi-field fixed-bed reactor series
Base fast-thermal PLR-SCR100 (single thermal field) / Resistive-heat reactor PLR RH
High-efficiency photothermal PLR-SCR100L (thermal + light) / Standard reactor PLR RS
High-efficiency thermal + microwave PLR-SCR100LM (thermal + microwave) / Resistive-heat reactor PLR RH
Rapid (thermal, light, microwave) full-package PLR-SCR100A (thermal + light + microwave) / Multi-function reactor PLR RMF
Choose one of four
Light source model Tri-unit annular LED light source
PLS-LCC — wavelength (optional: 365 nm, 380 nm, 405 nm, 420 nm, 760 nm)
Others customizable
Number of gas inlets Default 3 channels, 4 channels optional
Default N2 calibration, range 100 mL/min
Others customizable
Number of liquid inlets Default none, 1 channel optional
Flow range 0.001~2 mL/min
Others customizable
Operating temperature & pressure Device operating parameters: 3 MPa / 600℃, pressure accuracy 0.2% F.S., temperature stability ±1℃
Reactor usage requirements: pressure ≤ 3 MPa (300℃) / pressure ≤ 1 MPa (600℃)
 
Preheater Preheating, premixing, vaporization functions
Default 300℃, maximum 400℃
 
Condenser Liquid storage volume ≤ 50 mL, removable, 10 mm stepped (barbed) connector  
Device interfaces Gas interface: 1/8’ ferrule; Electrical interface: three-pin socket Piping not included
Power supply 220V / 10A, device maximum power < 2.2 kW Must be grounded
Device dimensions 700 mm × 800 mm × 480 mm (W × H × D) Other sizes customizable
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